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Chemical name: (S)-2-Azido-6-[(allyloxycarbonyl)amino]hexanoic acid dicyclohexylamine // Synonyms: N3-Lys(Alloc), Azido-Lys(Alloc)-OH, 2-azido-6-(allyloxycarbonyl)amino-hexanoic acid (S), alpha-Azido-epsilon-Alloc-L-lysine, (S)-2-Azido-6-(Alloc-amino)caproic acid
|Molecular weight:||256,26*181,32 g/mol|
All and Alloc are fully compatible with Fmoc/tBu and Boc/Bzl strategies, as well as with Z protecting groups.
Chinese Chemical Letters 2009; 20: 127-130; DOI:10.1016/j.cclet.2008.11.002.
Mild non-transition metal catalyzed deprotection of N-allyloxycarbonyl amines; Ronald H. Szumigala, Jr., Ekama Onofiok, Sandor Karady, Joseph D. Armstrong III, and Ross A. Miller; Tetrahedron Letters 2005; 46: 4403-4405. DOI: 10.1016/j.tetlet.2005.04.064.
Allylic Protecting Groups and Their Use in a Complex Environment. Part II: Allylic Protecting Groups and their Removal through Catalytic Palladium -Allyl Methodology; Franois Guib; Tetrahedron 1998; 54: 2967-3042.
Selective Cleavage of the Allyl and Allyloxycarbonyl Groups through Palladium-Catalyzed Hydrostannolysis with Tributyltin Hydride. Application to the Selective Protection-Deprotection of Amino Acid Derivatives and in Peptide Synthesis; O. Dangles, F. Guib, G. Balavoine; S. Lavielle, A. Marquet; J. Org. Chem. 1987; 52(22): 4984-4993.
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